3-碘-1-(苯磺酰)吲哚合成路线 （共 24 条）
反应条件
ethylmagnesium bromide in tetrahydrofuran
1.) 0 deg C, 30 min, r.t., 30 min; 2.) r.t., overnight;
参考文献
Kondo, Yoshinori; Yoshida, Akihiro; Sato, Shuichiroh; Sakamoto, Takao
Heterocycles, 1996 , vol. 42, # 1 p. 105 - 108
反应条件
[Fe(II)(C5H5)(C5H4PPh2)]; tris-(dibenzylideneacetone)dipalladium(0) in 1,4-dioxane
Substitution; Cyanation; 4 h; Heating;
参考文献
Sakamoto, Takao; Ohsawa, Kazutoshi
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 16 p. 2323 - 2326
反应条件
1: 96 percent / LDA; I2
2: 85 percent / P(o-tolyl)3; K2CO3 / Pd(OAc)2 / acetone; H2O / 5 h / 70 °C
3: 95 percent / Mg / methanol
View Scheme
参考文献
Liu; Gribble
Tetrahedron Letters, 2000 , vol. 41, # 45 p. 8717 - 8721
反应条件
1: CuI; Et3N / Pd(PPh3)4
2: K2CO3 / methanol
View Scheme
参考文献
Tanaka, Katsunori; Kobayashi, Toyoharu; Mori, Hajime; Katsumura, Shigeo
Journal of Organic Chemistry, 2004 , vol. 69, # 18 p. 5906 - 5925
