2-碘-1-(4-甲氧基苯基)-乙酮合成路线 (共 24 条)
反应条件
dimethyl sulfoxide; copper(II) oxide T=65°C; 2.5 h;
参考文献
Yin, Guodong; Zhou, Baohan; Meng, Xianggao; Wu, Anxin; Pan, Yuanjiang
Organic Letters, 2006 , vol. 8, # 11 p. 2245 - 2248
反应条件
air; triethylamine in acetone 5 h; Irradiation;
参考文献
Chai, Wen; Takeda, Akihiro; Hara, Makoto; Ji, Shun-Jun; Horiuchi, C. Akira
Tetrahedron, 2005 , vol. 61, # 9 p. 2453 - 2463
反应条件
in dimethyl sulfoxide; acetonitrile T=20°C; 1 h;
参考文献
Samakkanad, Natthapol; Katrun, Praewpan; Techajaroonjit, Thanachart; Hlekhlai, Sornsiri; Pohmakotr, Manat; Reutrakul, Vichai; Jaipetch, Thaworn; Soorukram, Darunee; Kuhakarn, Chutima
Synthesis (Germany), 2012 , vol. 44, # 11 art. no. SS-2012-N0148-OP, p. 1693 - 1699
反应条件
iodine; copper(II) oxide in ethanol T=78°C;
参考文献
Zhu, Yan-Ping; Yuan, Jing-Jing; Zhao, Qin; Lian, Mi; Gao, Qing-He; Liu, Mei-Cai; Yang, Yan; Wu, An-Xin
Tetrahedron, 2012 , vol. 68, # 1 p. 173 - 178
反应条件
potassium phosphate Rap-Stoermer reaction; 0.0333333 h; microwave irradiation;
参考文献
Rao, Maddali L.N.; Awasthi, Dheeraj K.; Banerjee, Debasis
Tetrahedron Letters, 2007 , vol. 48, # 3 p. 431 - 434
反应条件
1: p-TsOH / methanol / 3 h / 25 °C 2: AgBF4 / methanol / 0.25 h / 15 °C 3: 92 percent / aq. NaOH / methanol / 4 h / Ambient temperature View Scheme
参考文献
Giordano, Claudio; Castaldi, Graziano; Casagrande, Francesco; Belli, Aldo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 11 p. 2575 - 2582
反应条件
hydrogenchloride; ammonium nitrate; iodine; oxygen in water; acetonitrile T=60°C; 24 h; Green chemistry; regioselective reaction;
参考文献
Prebil, Rok; Stavber, Stojan
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 6 p. 1266 - 1274
反应条件
1: p-TsOH / methanol / 3 h / 25 °C 2: AgBF4 / methanol / 0.25 h / 15 °C View Scheme
参考文献
Giordano, Claudio; Castaldi, Graziano; Casagrande, Francesco; Belli, Aldo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 11 p. 2575 - 2582
反应条件
air; triethylamine in acetone 5 h; Irradiation;
参考文献
Tetrahedron, , vol. 61, # 9 p. 2453 - 2463
反应条件
NH4I; Oxonereg; in methanol
T=20°C; 22 h;
参考文献
Marri, Mahender Reddy; MacHarla, Arun Kumar; Peraka, Swamy; Nama, Narender
Tetrahedron Letters, 2011 , vol. 52, # 49 p. 6554 - 6559