N-苄基-4-溴苯甲酰胺合成路线 （共 14 条）
反应条件
trichloromonobromomethane; 4-(diphenylphosphino)-benzyltrimethylammonium bromide; triethylamine in tetrahydrofuran T=60°C; 6 h; Inert atmosphere;
参考文献
Kawagoe, Yuhsuke; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2013 , vol. 69, # 19 p. 3971 - 3977
反应条件
1: 4-bromo-benzoyl chloride With pyridine; 2-oxo-1,2-dihydropyrimidine in dichloromethane 0.05 h; microwave irradiation; 2: benzylamine in dichloromethane 0.05 h; microwave irradiation;
参考文献
Petricci, Elena; Mugnaini, Claudia; Radi, Marco; Corelli, Federico; Botta, Maurizio
Journal of Organic Chemistry, 2004 , vol. 69, # 23 p. 7880 - 7887
反应条件
tert.-butylhydroperoxide; manganese(IV) oxide in water; acetonitrile T=80°C; 48 h;
参考文献
Vanjari, Rajeshwer; Guntreddi, Tirumaleswararao; Singh, Krishna Nand
Organic Letters, 2013 , vol. 15, # 18 p. 4908 - 4911
反应条件
boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid in chloroform T=20°C; 4 h;
参考文献
An, Gwang-Il; Rhee, Hakjune
Synlett, 2003 , # 6 p. 876 - 878
反应条件
phenyl silane; triphenylphosphine in toluene T=20 - 110°C; Staudinger Azide Reduction; 19 h; Inert atmosphere; chemoselective reaction;
参考文献
Kosal, Andrew D.; Wilson, Erin E.; Ashfeld, Brandon L.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 48 p. 12036 - 12040
Angew. Chem., 2012 , vol. 124, # 48 p. 12202 - 12206
反应条件
1: p-BrC6H4CH(=NOH) With [{(η5-C5Me5)IrCl}2(μ-Cl)2]; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2 in toluene T=130°C; 3 h; Inert atmosphereSchlenk techniqueGreen chemistry; 2: benzyl alcohol With caesium carbonate in toluene T=130°C; 12 h; Inert atmosphereSchlenk techniqueGreen chemistry;
参考文献
Li, Feng; Qu, Panpan; Ma, Juan; Zou, Xiaoyuan; Sun, Chunlou
ChemCatChem, 2013 , vol. 5, # 8 p. 2178 - 2182
反应条件
magnetite nanoparticle-supported sulfonic acid in neat (no solvent) T=90°C; Ritter Amidation; 4 h;
参考文献
Green Chemistry, , vol. 15, # 7 p. 1895 - 1899
反应条件
palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine in tetrahydrofuran 13 h; Reflux;
参考文献
Wei, Ren; Yamane, Motoki
Journal of Organic Chemistry, 2009 , vol. 74, # 21 p. 8332 - 8335
反应条件
tri(n-propyl)amine; tetraethylammonium chloride in diethylene glycol dimethyl ether T=150°C; 1 h; Inert atmosphere;
参考文献
Ren, Wei; Yamane, Motoki
Journal of Organic Chemistry, 2010 , vol. 75, # 24 p. 8410 - 8415
反应条件
tributyl-amine in diethylene glycol dimethyl ether 0.5 h; Inert atmosphere;
参考文献
Ren, Wei; Yamane, Motoki
Journal of Organic Chemistry, 2010 , vol. 75, # 9 p. 3017 - 3020
