1-正丁基-4-[(4-正丁基苯基)乙炔基]苯合成路线 (共 7 条)
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=100°C; Stille coupling; 2 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 52, # 16 p. 1960 - 1963
反应条件
dysprosium in N,N-dimethyl acetamide T=80°C; 3 h; Inert atmosphere;
参考文献
Organometallics, , vol. 30, # 7 p. 2026 - 2030
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; palladium dichloride; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in dimethyl sulfoxide T=120°C; 24 h; Inert atmosphere;
参考文献
RSC Advances, , vol. 4, # 26 p. 13738 - 13741
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); water; 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran Sonogashira Cross-Coupling; Inert atmosphereReflux;
参考文献
Organic Letters, , vol. 16, # 6 p. 1594 - 1597
反应条件
diethyl ether; ammonia; KNH2
参考文献
Journal of the American Chemical Society, , vol. 56, p. 132
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine T=60°C; Inert atmosphereSchlenk technique;
参考文献
Chemical Communications, , vol. 49, # 86 p. 10121 - 10123
反应条件
perfluorodecahydronaphthalene; oxygen; palladium diacetate; zinc(II) chloride in N,N-dimethyl acetamide
T=60°C; P=760.051 Torr; 24 h; sealed tube;
参考文献
Wen, Yanmei; Zhu, Shifa; Jiang, Huanfeng; Wang, Azhong; Chen, Zhenwang
Synlett, 2011 , # 7 p. 1023 - 1027