1,3-双(α-羟基六氟异丙基)苯合成路线 （共 5 条）
反应条件
aluminium trichloride T=50 - 54°C; 6 h;
参考文献
Sepiol, Janiusz; Soulen, Robert L.
Journal of Fluorine Chemistry, 1984 , vol. 24, p. 61 - 74
反应条件
aluminium trichloride T=50 - 54°C; 5 h;
参考文献
Journal of Fluorine Chemistry, , vol. 24, p. 61 - 74
反应条件
sulfuric acid; iodine
7 h; Ambient temperature;
参考文献
Fujiki, Kanji; Kashiwagi, Mitsuyoshi; Miyamoto, Hideyuki; Sonoda, Akinari; Ichikawa, Junji; et al.
Journal of Fluorine Chemistry, 1992 , vol. 57, p. 307 - 321
反应条件
sulfur trioxide; iodine in sulfuric acid
参考文献
Soulen, Robert L.; Griffith, James R.
Journal of Fluorine Chemistry, 1989 , vol. 44, p. 203 - 210
反应条件
1: 1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene With sodium hydride in N,N-dimethyl-formamide
T=-20 - -10°C;
2: methanesulphonic acid methyl ester in N,N-dimethyl-formamide
T=20°C; 12 h;
参考文献
Rabai, Jozsef; Szabo, Denes; Borbas, Eszter K.; Koevesi, Istvan; Koevesdi, Istvan; Csampai, Antal; Goemoery, Agnes; Pashinnik, Valeriy E.; Shermolovich, Yuriy G.
Journal of Fluorine Chemistry, 2002 , vol. 114, # 2 p. 199 - 207
