N-甲基-N-亚硝基对甲苯磺酰胺合成路线 (共 111 条)
反应条件
sodium bis(2-ethylhexyl)-sulfosuccinate in 2,2,4-trimethylpentane T=25°C; also in water; Rate constant;
参考文献
Castro, Albino; Leis, J. Ramon; Pena, M. Elena
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1861 - 1866
反应条件
methanol; ammonium hydroxide in dichloromethane 168 h; Ambient temperature; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 49, # 18 p. 3322 - 3327
反应条件
1: With potassium hydroxide in methanol; water T=0°C; 2: With acetic acid in methanol; water
参考文献
Meyer-Wilmes, Imelda; Gerke, Ralf; Fitjer, Lutz
Tetrahedron, 2009 , vol. 65, # 8 p. 1689 - 1696
反应条件
potassium hydroxide in water T=20°C; 1.16667 h; Concentration;
参考文献
Pinho, Vagner D.; Gutmann, Bernhard; Miranda, Leandro S. M.; De Souza, Rodrigo O. M. A.; Kappe, C. Oliver
Journal of Organic Chemistry, 2014 , vol. 79, # 4 p. 1555 - 1562
反应条件
potassium hydroxide in tetrahydrofuran; methanol; water T=20°C;
参考文献
Mastronardi, Federica; Gutmann, Bernhard; Oliver Kappe
Organic Letters, 2013 , vol. 15, # 21 p. 5590 - 5593
反应条件
tetradecyltrimethylammonium bromide in various solvents T=25°C; Kinetics;
参考文献
Garcia-Rio, Luis; Hervella, Pablo
Chemistry - A European Journal, 2006 , vol. 12, # 32 p. 8284 - 8295
反应条件
in 1,4-dioxane; water T=25°C; var. total amine concentrations; Rate constant;
参考文献
Garcia-Rio, Luis; Iglesias, Emilia; Leis, J. Ramon; Pena, M. Elena; Rios, Ana
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 1 p. 29 - 37
反应条件
in 1,4-dioxane; water T=25°C; Rate constant;
参考文献
Garcia-Rio, Luis; Iglesias, Emilia; Leis, J. Ramon; Pena, M. Elena; Rios, Ana
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 1 p. 29 - 37
反应条件
potassium hydroxide in methanol; diethyl ether byproducts: N2; addn. of MeOH to KOH (65°C), dropwise addn. of diazald in ether, refluxing), addn. of suspn. of HgCl2 in ether (0°C, ice-bath), pptn.; removal of solvent (evapn.), recrystn. (MeOH); elem. anal.;
参考文献
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, , vol. 42, # 4 p. 427 - 430
反应条件
potassium hydroxide in methanol; water T=20°C; 1.16667 h;
参考文献
Pinho, Vagner D.; Gutmann, Bernhard; Miranda, Leandro S. M.; De Souza, Rodrigo O. M. A.; Kappe, C. Oliver
Journal of Organic Chemistry, 2014 , vol. 79, # 4 p. 1555 - 1562