反应条件
1: 76 percent / PCl5 / 12 h / 20 °C
2: 53 percent / KOH / ethanol / Heating
3: 1.) MeI, Li / 1.) Et2O, 20 deg C, 1 h; 2.) 20 deg C, 12 h
4: 84 percent / CaCl2, CuCl, Cu, 12N HCl / diethyl ether; petroleum ether / 1 h / 5 °C
5: 1.) Mg / 1.) Et2O; 2.) 12 h, RT; 2 h, reflux
View Scheme
参考文献
Mesnard, Danielle; Bernadou, Francoise; Miginiac, Leone
Journal of Chemical Research, Miniprint, 1981 , # 9 p. 3216 - 3245
