5-甲酰基-3-甲基-1H-吡咯-2,4-二甲酸合成路线 (共 9 条)
反应条件
potassium hydroxide in water
2 h; Heating;
参考文献
Brittain, Judith M.; Jones, R. Alan; Jones, Richard O.; King, Trevor J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2656 - 2661
反应条件
potassium hydroxide
Heating;
参考文献
Brittain, Judith M.; Jones, R. Alan; Jones, Richard O.; King, Trevor J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2656 - 2661
反应条件
potassium hydroxide
4 h; Heating;
参考文献
Brittain, Judith M.; Jones, R. Alan; Jones, Richard O.; King, Trevor J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2656 - 2661
反应条件
potassium hydroxide
Heating;
参考文献
Brittain, Judith M.; Jones, R. Alan; Jones, Richard O.; King, Trevor J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2656 - 2661
反应条件
1: 67 percent / sulphuryl chloride / acetic acid / 0.5 h / 50 °C
2: 64 percent / 6percent aq. KOH / H2O / 2 h / Heating
View Scheme
参考文献
Brittain, Judith M.; Jones, R. Alan; Jones, Richard O.; King, Trevor J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2656 - 2661
反应条件
1: 61 percent / sulphuryl chloride / acetic acid / 0.5 h / 50 °C
2: 83 percent / aq. KOH / Heating
View Scheme
参考文献
Brittain, Judith M.; Jones, R. Alan; Jones, Richard O.; King, Trevor J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2656 - 2661
参考文献
Fischer; Ernst
Justus Liebigs Annalen der Chemie, 1926 , vol. 447, p. 153
反应条件
1: 72 percent
2: 79 percent / 6percent aq. KOH / 4 h / Heating
View Scheme
参考文献
Brittain, Judith M.; Jones, R. Alan; Jones, Richard O.; King, Trevor J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2656 - 2661
反应条件
1: 55 percent / sulphuryl chloride
2: 86 percent / aq. KOH / Heating
View Scheme
参考文献
Brittain, Judith M.; Jones, R. Alan; Jones, Richard O.; King, Trevor J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2656 - 2661