反应条件
1: 1.) Mg, 2.) POCl3 / 1.) THF, RT, 1 h, 2.) 1 h
2: 86 percent / KMnO4 / H2O / 16 h / Ambient temperature
3: 1.) BBr3, 2.) H2O / 1.) CH2Cl2, from -78 deg C to RT, 24 h, 2.) reflux
View Scheme
参考文献
Friedrichsen, Bernard P.; Powell, Douglas R.; Whitlock, Howard W.
Journal of the American Chemical Society, 1990 , vol. 112, # 24 p. 8931 - 8941
