3,4-二氢异喹啉-2(1H)-胺盐酸盐合成路线 （共 5 条）
反应条件
hydrogenchloride; sodium disulfite in sodium hydroxide; ethanol
T=62°C; 4 h;
参考文献
Powell, Burwell F.; Overberger, C. G.; Anselme, J.-P.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 121 - 128
反应条件
hydrogenchloride
T=40°C;
参考文献
Salman, Mohammad; Ray, Suprabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 477 - 479
反应条件
1: 54 percent / conc. HCl, NaNO2 / H2O / 2 h / 75 °C
2: 54 percent / 1.) sodium hydrosulfite, 2.) HCl / ethanol; aq. NaOH / 4 h / 62 °C
View Scheme
参考文献
Powell, Burwell F.; Overberger, C. G.; Anselme, J.-P.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 121 - 128
反应条件
1: 53 percent / triethylamine / dimethylformamide / 50 - 60 °C
2: 43 percent / conc. HCl / 40 °C
View Scheme
参考文献
Salman, Mohammad; Ray, Suprabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 477 - 479
反应条件
acetic acid
Heating;
参考文献
Salman, Mohammad; Ray, Suprabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 477 - 479
