2,6-二溴-3-甲氧基吡啶合成路线 （共 7 条）
反应条件
1: 45 percent / nitric acid, conc. sulfuric acid / 2 h / 60 - 65 °C 2: 63 percent / hydrazine hydrate / Pd/C / ethanol / 0.5 h / Heating View Scheme
参考文献
Clark, Gary J.; Deady, Leslie W.
Australian Journal of Chemistry, 1981 , vol. 34, # 4 p. 927 - 932
反应条件
potassium carbonate in dimethyl sulfoxide
1 h; Heating;
参考文献
Clark, Gary J.; Deady, Leslie W.
Australian Journal of Chemistry, 1981 , vol. 34, # 4 p. 927 - 932
反应条件
1: 44 percent / bromine, aq. NaOH / 1.) 0 deg C, 0.5 h, 2.) RT, 2 h
2: 79 percent / potassium carbonate / dimethylsulfoxide / 1 h / Heating
View Scheme
参考文献
Clark, Gary J.; Deady, Leslie W.
Australian Journal of Chemistry, 1981 , vol. 34, # 4 p. 927 - 932
反应条件
sulfuric acid; nitric acid
T=60 - 65°C; 2 h;
参考文献
Clark, Gary J.; Deady, Leslie W.
Australian Journal of Chemistry, 1981 , vol. 34, # 4 p. 927 - 932
反应条件
1: 45 percent / nitric acid, conc. sulfuric acid / 2 h / 60 - 65 °C
2: 44 percent / H2 / platinum oxide / ethanol / 760 Torr
View Scheme
参考文献
Clark, Gary J.; Deady, Leslie W.
Australian Journal of Chemistry, 1981 , vol. 34, # 4 p. 927 - 932
反应条件
1: 45 percent / nitric acid, conc. sulfuric acid / 2 h / 60 - 65 °C
2: 95 percent / sodium methoxide / methanol / 20 h
View Scheme
参考文献
Clark, Gary J.; Deady, Leslie W.
Australian Journal of Chemistry, 1981 , vol. 34, # 4 p. 927 - 932
反应条件
1: 45 percent / nitric acid, conc. sulfuric acid / 2 h / 60 - 65 °C
2: 95 percent / sodium methoxide / methanol / 20 h
3: hydrazine hydrate / Pd/C / ethanol / 0.5 h / Heating
View Scheme
参考文献
Clark, Gary J.; Deady, Leslie W.
Australian Journal of Chemistry, 1981 , vol. 34, # 4 p. 927 - 932
