2,3-二甲氧基-6-硝基吡啶合成路线 （共 9 条）
反应条件
in methanol; dimethyl sulfoxide T=20 - 35°C; 49.5 h;
参考文献
BIOLIPOX AB
Patent: WO2007/51981 A1, 2007 ;
Location in patent: Page/Page column 56 ;
反应条件
in dimethyl sulfoxide T=20 - 35°C; 49.5 h;
参考文献
BIOLIPOX AB
Patent: WO2007/51982 A1, 2007 ;
Location in patent: Page/Page column 48 ;
反应条件
sodium in dimethyl sulfoxide T=30°C; 2 h;
参考文献
Clark, Gary J.; Deady, Leslie W.
Australian Journal of Chemistry, 1981 , vol. 34, # 4 p. 927 - 932
反应条件
sodium methylate Heating;
参考文献
Dehmlow, Eckehard V.; Schulz, Hans-Joachim
Journal of Chemical Research, Miniprint, 1987 , # 11 p. 2951 - 2973
反应条件
1: 48 percent / nitric acid, conc. sulfuric acid / 0.5 h / Heating 2: 81 percent / sodium / dimethylsulfoxide / 2 h / 30 °C View Scheme
参考文献
Australian Journal of Chemistry, , vol. 34, # 4 p. 927 - 932
反应条件
1: 1) KOH / 1) DMSO, 50 deg C, 20 min, 2) DMSO, 50 deg C, 30 min 2: 67.9 percent / 30percent H2O2 / acetic anhydride / Ambient temperature 3: 64.4 percent / conc. H2SO4, 100percent HNO3 / Ambient temperature 4: 34 percent / PCl3 / CHCl3 / 1 h / Heating 5: 80.4 percent / NaOMe / Heating View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 11 p. 2951 - 2973
反应条件
1: 67.9 percent / 30percent H2O2 / acetic anhydride / Ambient temperature 2: 64.4 percent / conc. H2SO4, 100percent HNO3 / Ambient temperature 3: 34 percent / PCl3 / CHCl3 / 1 h / Heating 4: 80.4 percent / NaOMe / Heating View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 11 p. 2951 - 2973
反应条件
1: 64.4 percent / conc. H2SO4, 100percent HNO3 / Ambient temperature 2: 34 percent / PCl3 / CHCl3 / 1 h / Heating 3: 80.4 percent / NaOMe / Heating View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 11 p. 2951 - 2973
反应条件
1: 34 percent / PCl3 / CHCl3 / 1 h / Heating 2: 80.4 percent / NaOMe / Heating View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 11 p. 2951 - 2973
