2-三氟甲基-5,6,7,8-四氢-[1,6]萘啶合成路线 （共 3 条）
反应条件
palladium 10 on activated carbon; hydrogen in methanol
参考文献
Johnson, Russell J.; O'Mahony, Donogh J. R.; Edwards, William T.; Duncton, Matthew A. J.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 8 p. 1358 - 1366
反应条件
1: 1,4-dioxane / 20 °C / |Inert atmosphere
2: ammonium acetate / 3 h / |Reflux
3: hydrogen; palladium 10 on activated carbon / methanol
View Scheme
参考文献
Johnson, Russell J.; O'Mahony, Donogh J. R.; Edwards, William T.; Duncton, Matthew A. J.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 8 p. 1358 - 1366
反应条件
1: benzene / 2.16 h / 20 °C / |Dean-Stark; |Inert atmosphere; |Reflux
2: 1,4-dioxane / 20 °C / |Inert atmosphere
3: ammonium acetate / 3 h / |Reflux
4: hydrogen; palladium 10 on activated carbon / methanol
View Scheme
参考文献
Johnson, Russell J.; O'Mahony, Donogh J. R.; Edwards, William T.; Duncton, Matthew A. J.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 8 p. 1358 - 1366
