甲基2-(2-甲基苯基)丙酸酯合成路线 （共 17 条）
反应条件
sodium hydroxide in methanol 2 h; Heating;
参考文献
Matsumoto; Ishida; Yoshida; Terao; Takeda; Asakawa
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 7 p. 1721 - 1726
反应条件
sodium hydrogencarbonate in N,N-dimethyl-formamide
T=20°C; 48 h;
参考文献
Brudeli, Bjarne; Moltzau, Lise Roman; Nguyen, Cam H.T.; Andressen, Kjetil Wessel; Nilsen, Nils Olav; Levy, Finn Olav; Klaveness, Jo
European Journal of Medicinal Chemistry, 2013 , vol. 64, p. 629 - 637
反应条件
0.17percent Pd-P-OP/LSI-600 catalyst in toluene
T=80°C; P=22502.3 Torr; 3.5 h; Autoclave;
参考文献
He, Zhenhong; Hou, Zhenshan; Luo, Yanping; Dilixiati, Yierxiati; Eli, Wumanjiang
Catalysis Science and Technology, 2014 , vol. 4, # 4 p. 1092 - 1103
反应条件
sulfuric acid; 3-[4-(diacetoxyiodo)phenoxy]-1-propyl-N,N,N-trimethylammonium 4-methylbenzenesulfonate
T=60°C; 3 h; Inert atmosphere;
参考文献
Iinuma, Masataka; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2013 , vol. 69, # 14 p. 2961 - 2970
反应条件
1: methyl (4-methylphenyl)acetate With potassium hydride in tetrahydrofuran
T=0 - 20°C;
2: methyl iodide in tetrahydrofuran
T=20°C; 14 h; Further stages.;
参考文献
Natarajan, Arunkumar; Ng, Danny; Yang, Zhe; Garcia-Garibay, Miguel A.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 34 p. 6485 - 6487
反应条件
NiBr2bipy; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide
T=70°C; i = 250 mA, nickel-sponge cathode;
参考文献
Durandetti, Muriel; Nedelec, Jean-Yves; Perichon, Jacques
Journal of Organic Chemistry, 1996 , vol. 61, # 5 p. 1748 - 1755
反应条件
tetrachloromethane; triphenylphosphine in dichloromethane
15 h; Ambient temperature;
参考文献
Sonawane, H. R.; Nanjundiah, B. S.; Kulkarni, D. G.; Ahuja, Jaimala R.
Tetrahedron, 1988 , vol. 44, # 23 p. 7319 - 7324
反应条件
sulfuric acid; trimethyl orthoformate
0.333333 h; Heating;
参考文献
Justik, Michael W.
Tetrahedron Letters, 2007 , vol. 48, # 17 p. 3003 - 3007
反应条件
zinc dibromide in toluene
T=115°C; 1.5 h;
参考文献
Castaldi, Graziano; Belli, Aldo; Uggeri, Fulvio; Giordano, Claudio
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4658 - 4661
反应条件
perchloric acid; thallium(III) nitrate
T=50°C; 3 h;
参考文献
Yamauchi, Takayoshi; Nakao, Kenji; Fujii, Kyoichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1255 - 1258
