反应条件
water; ammonium chloride in diethyl ether
to soln. of Bu3SnCHCl(OEt) in anhyd. Et2O added dropwise soln. of CH2CHCH2MgBr in anhyd. Et2O at 0 °C, after 1 h at 0 °C added satd. aq. soln. of NH4Cl; extd. (Et2O), org. layer dried (MgSO4), distd. in vac. or chromd. (SiO2, pentane);
参考文献
Quintard, Jean-Paul; Elissondo, Bernard; Hattich, Thomas; Pereyre, Michel
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 149 - 162
