7-氧代双环[2.2.1]庚烷-1-甲酰氯合成路线 (共 5 条)
反应条件
multistep reaction; cata. decarbonylation with chlorocarbonylbis(triphenylphosphan)rhodium; Product distribution;
参考文献
Liebigs Annalen der Chemie, , # 8 p. 1394 - 1406
反应条件
multistep reaction; cata. decarbonylation with chlorocarbonylbis(triphenylphosphan)rhodium; Product distribution;
参考文献
Liebigs Annalen der Chemie, , # 8 p. 1394 - 1406
反应条件
multistep reaction; cata. decarbonylation with chlorocarbonylbis(triphenylphosphan)rhodium; Product distribution;
参考文献
Kirmse, Wolfgang; Sandkuehler, Peter
Liebigs Annalen der Chemie, 1981 , # 8 p. 1394 - 1406
反应条件
multistep reaction; cata. decarbonylation with chlorocarbonylbis(triphenylphosphan)rhodium; Product distribution;
参考文献
Liebigs Annalen der Chemie, , # 8 p. 1394 - 1406
反应条件
1: 91 percent / p-TsOH / methanol / 12 h / Ambient temperature
2: 86 percent / 20 percent methanolic KOH / 4 h / Heating
3: 36 percent / HgO/Br2, CH2Br2 / 1 h / 60 - 80 °C
4: 85 percent / 50 percent H2SO4 / diethyl ether / 6 h / Ambient temperature
5: 86 percent / 1 N LiOH / 6 h / 80 °C
View Scheme
参考文献
Kirmse, Wolfgang; Sandkuehler, Peter
Liebigs Annalen der Chemie, 1981 , # 8 p. 1394 - 1406