反应条件
1: 99 percent / NaN3, tricaprylmethylammonium chloride / H2O / 14 h / 60 °C
2: hydroquinone or hydroquinone methyl ether / 1 mol-percent Re2S7 / 13.5 h / 90 °C / a) Re2S7, hydroquinone or hydroquinone methyl ether, 80 deg C, 24 h, b) MoS3, HCl, hydroquinone, 80 deg C, 72 h
3: HCl / diethyl ether / 46 h / Ambient temperature
View Scheme
参考文献
Effenberger, Franz; Beisswenger, Thomas
Chemische Berichte, 1984 , vol. 117, # 4 p. 1497 - 1512
