9-氯-9,10-二氢-9,10-[1,2]苯并蒽合成路线 （共 9 条）
反应条件
Li (2percent Na) in diethyl ether 2 h; Heating;
参考文献
Molle, G.; Bauer, P.; Dubois, J. E.
Journal of Organic Chemistry, 1983 , vol. 48, # 18 p. 2975 - 2981
反应条件
maleic anhydride; carbon; isopentyl nitrite
1) dichloroethane, THF, reflux, 2) toluene, reflux, 30 min;
参考文献
Molle, G.; Bauer, P.; Dubois, J. E.
Journal of Organic Chemistry, 1983 , vol. 48, # 18 p. 2975 - 2981
反应条件
1: PhNO, aq. KOH / ethanol
2: SnCl2, AcOH, aq. HCl
3: HCl, EtONO / methanol
View Scheme
参考文献
Theilacker,W.; Beyer,K.-H.
Chemische Berichte, 1961 , vol. 94, p. 2968 - 2977
反应条件
hydrogenchloride; EtO-NO in methanol
参考文献
Theilacker,W.; Beyer,K.-H.
Chemische Berichte, 1961 , vol. 94, p. 2968 - 2977
反应条件
1: petroleum ether
2: Al(OiPr)3 / propan-2-ol
3: POCl3, PCl3
View Scheme
参考文献
Theilacker,W. et al.
Chemische Berichte, 1960 , vol. 93, p. 1658 - 1681
反应条件
1: SnCl2, AcOH, aq. HCl
2: HCl, EtONO / methanol
View Scheme
参考文献
Theilacker,W.; Beyer,K.-H.
Chemische Berichte, 1961 , vol. 94, p. 2968 - 2977
反应条件
1: PhNHOH, aq. KOH / ethanol
2: PhNO, aq. KOH / ethanol
3: SnCl2, AcOH, aq. HCl
4: HCl, EtONO / methanol
View Scheme
参考文献
Theilacker,W.; Beyer,K.-H.
Chemische Berichte, 1961 , vol. 94, p. 2968 - 2977
反应条件
in tetrahydrofuran
T=0°C; Product distribution; Further Variations:Reagents;
参考文献
Adcock; Clark; Trout
Journal of Organic Chemistry, 2001 , vol. 66, # 10 p. 3362 - 3371
反应条件
triethylamine in cyclohexane
10 h; Ambient temperatureIrradiation;
参考文献
Toda, Takashi; Minabe, Masahiro; Yoshida, Masaaki; Tobita, Keisuke
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1297 - 1300
