N-(3,5-二甲氧基苯基)乙酰胺合成路线 （共 8 条）
反应条件
1: With Schwartz's reagent in tetrahydrofuran T=20°C; 0.05 h; Inert atmosphere; 2: With water in tetrahydrofuran Inert atmosphere; chemoselective reaction;
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 2 p. 261 - 264
反应条件
pyridine
T=0 - 20°C;
参考文献
Duan, Hongliang; Zheng, Jin; Lai, Qinglin; Liu, Zheng; Tian, Guanghui; Wang, Zhen; Li, Jianfeng; Shen, Jingshan
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 10 p. 2777 - 2779
参考文献
Dean; Whalley
Journal of the Chemical Society, 1954 , p. 4638,4640
反应条件
triethylamine in tetrahydrofuran
T=5 - 20°C;
参考文献
Beharry, Andrew A.; Sadovski, Oleg; Woolley, G. Andrew
Journal of the American Chemical Society, 2011 , vol. 133, # 49 p. 19684 - 19687
反应条件
1: aqueous dioxane
2: aqueous NaOH
View Scheme
参考文献
Sorm; Novotny
Chemicke Listy, 1954 , vol. 49, p. 901,907
Collection of Czechoslovak Chemical Communications, 1955 , vol. 20, p. 1206,1212
Chem. Zentralbl., 1955 , vol. 126, p. 13244
反应条件
methanol; diethyl ether
参考文献
Sorm; Novotny
Chemicke Listy, 1954 , vol. 49, p. 901,907
Collection of Czechoslovak Chemical Communications, 1955 , vol. 20, p. 1206,1212
Chem. Zentralbl., 1955 , vol. 126, p. 13244
参考文献
Sorm; Novotny
Chemicke Listy, 1954 , vol. 49, p. 901,907
Collection of Czechoslovak Chemical Communications, 1955 , vol. 20, p. 1206,1212
Chem. Zentralbl., 1955 , vol. 126, p. 13244
反应条件
1: 92 percent / BF3*Et2O / dioxane / Heating
2: H2O, alkali
3: 94 percent / Cu(OAc)2 / propan-2-ol
4: 91 percent / PPE
5: EtSNa / dimethylformamide
6: DDQ / 1,2-dichloro-benzene
View Scheme
参考文献
Anand; Selvapalam
Chemical Communications, 1996 , # 2 p. 199 - 200
