2,4,6-三碘苯-1,3,5-三羧酸合成路线 (共 2 条)
反应条件
1: With sodium hydroxide; water
T=90°C; 5 h;
2: With hydrogenchloride in water
pH=6 - 7;
3: With potassium permanganate; magnesium sulfate in water
2 h; Heating / reflux; Product distribution / selectivity;
参考文献
SCHERING AKTIENGESELLSCHAFT
Patent: WO2005/5362 A1, 2005 ;
Location in patent: Page/Page column 8-13 ;
反应条件
1: With potassium permanganate; sulfuric acid
T=40 - 50°C; 20 - 30 h; Acidic conditions;
2: With sodium hydroxide in water
T=20°C; Alkaline conditions;
3: With sodium hydroxide; potassium permanganate; sulfuric acid; water
Product distribution / selectivity; more than 3 stages;
参考文献
SCHERING AKTIENGESELLSCHAFT
Patent: WO2005/5363 A1, 2005 ;
Location in patent: Page/Page column 7-13 ;