联苯-4,4-二羧酸二甲酯合成路线 （共 64 条）
反应条件
NiCl2((PPh3)P)2; tetraethylammonium iodide; zinc in tetrahydrofuran T=67°C; 10 h; other solvents, temperature and time; other formulas and amounts of a catalyst; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 60, # 1 p. 176 - 185
反应条件
1: alkali; permanganate 2: PCl5 View Scheme
参考文献
Chemische Berichte, , vol. 32, p. 1053
反应条件
(i) Py, (ii) aq. NaOH, (iii) /BRN= 102415/; Multistep reaction;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 22, p. 140 - 152
反应条件
sodium hydroxide in ethanol; water 1 h; Reflux;
参考文献
Ol'khovik; Pap; Vasilevskii; Galinovskii; Tereshko
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 8 p. 1172 - 1179
反应条件
1-methyl-piperazine; sodium bis(2-methoxyethoxy)aluminium dihydride in toluene T=5°C; 3 h;
参考文献
Hagiya, Kazutake; Mitsui, Sunao; Taguchi, Hiroaki
Synthesis, 2003 , # 6 p. 823 - 828
参考文献
Tschitschibabin
Chemische Berichte, 1907 , vol. 40, p. 1818
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1907 , vol. 39, p. 934
反应条件
LiAlH4 in tetrahydrofuran; tetrahydrofuran-water; acetone
参考文献
ENIRICERCHE S.p.A.
Patent: EP469682 A1, 1992 ;
反应条件
LiAlH4 in tetrahydrofuran; ethanol; acetone
参考文献
Eniricerche S.p.A.
Patent: US5166380 A1, 1992 ;
反应条件
sulfuric acid; silver sulphate
T=80°C; 36 h;
参考文献
Kwong, Chi-Yuen; Chan, Tze-Lock; Chow, Hak-Fun; Lin, Shi-Chun; Leung, Man-Kit
Journal of the Chinese Chemical Society, 1997 , vol. 44, # 3 p. 211 - 224
反应条件
1: 99 percent / chlorosulfonic acid / 3 h / 130 - 155 °C
2: 97 percent / NaOH / 0.25 h / 315 - 320 °C
View Scheme
参考文献
Ol'khovik; Matveenko; Kalechits; Pap; Zenyuk
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 8 p. 1164 - 1168
