联苯-4,4-二羧酸二甲酯合成路线 (共 64 条)
反应条件
tetrabutylammomium bromide in N,N-dimethyl-formamide T=65°C; 21.5 h; electrochemical reduction;
参考文献
Tetrahedron Letters, , vol. 21, p. 631 - 634
反应条件
1: 2,6-lutidine, 4-dimethylaminopyridine / CH2Cl2 / 2 h / -30 - 25 °C 2: 85 percent / triethylamine, 1,3-bis(diphenylphosphino)propane, / Pd(OAc)2 / dimethylsulfoxide / 1 h / 70 °C View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 12 p. 904 - 905
反应条件
phosphorus pentachloride
参考文献
Chemische Berichte, , vol. 32, p. 1053
反应条件
NiCl2((PPh3)P)2; tetraethylammonium iodide; zinc in tetrahydrofuran 1.) r.t., 5 min, 2.) 67 deg C, 10 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 60, # 1 p. 176 - 185
反应条件
NiCl2((PPh3)P)2; tetraethylammonium iodide; zinc in tetrahydrofuran 1.) r.t., 5 min, 2.) 67 deg C, 5 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 60, # 1 p. 176 - 185
反应条件
potassium phosphate; zinc; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; potassium iodide in tetrahydrofuran T=67°C; 24 h; various solvents, temp., catalysts, base; also in the presence of halide; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 60, # 4 p. 1060 - 1065
反应条件
[2,2']bipyridinyl; manganese; trifluoroacetic acid; cobalt(II) dibromide in pyridine; N,N-dimethyl-formamide T=50°C; 3.5 h; Product distribution; Further Variations:ReagentsSolventsTemperatures;
参考文献
Amatore, Muriel; Gosmini, Corinne; Perichon, Jacques
European Journal of Organic Chemistry, 2005 , # 6 p. 989 - 992
反应条件
1: AlCl3 / CS2 2: Br2 / CHCl3 3: (i) Py, (ii) aq. NaOH, (iii) /BRN= 102415/ View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 22, p. 140 - 152
反应条件
1: Br2 / CHCl3 2: (i) Py, (ii) aq. NaOH, (iii) /BRN= 102415/ View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 22, p. 140 - 152
反应条件
Hg(II)-TFA 1.) RT, overnight, 2.) 75-100 deg C, 50-100 psig; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 50, # 23 p. 4601 - 4605