联苯-4,4-二羧酸二甲酯合成路线 (共 64 条)
反应条件
triethylamine; G0-C2 PAMAM dendrimer*PPh2*PdMe2 T=105°C; P=5171.62 Torr; 19 h;
参考文献
Antebi, Shlomo; Arya, Prabhat; Manzer, Leo E.; Alper, Howard
Journal of Organic Chemistry, 2002 , vol. 67, # 19 p. 6623 - 6631
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
反应条件
carbon tetrabromide; oxygen 48 h; Irradiation;
参考文献
Hirashima, Shin-Ichi; Nobuta, Tomoya; Tada, Norihiro; Miura, Tsuyoshi; Itoh, Akichika
Organic Letters, 2010 , vol. 12, # 16 p. 3645 - 3647
反应条件
triphenylphosphine; zinc; NiCl2((PPh3)P)2 in N,N-dimethyl-formamide T=80°C; 12 h;
参考文献
Journal of Organic Chemistry, , vol. 60, # 21 p. 6895 - 6903
反应条件
3-chloroprop-1-ene; trifluoroacetic acid; zinc; Co(2,2'-bipyridine)Br2 in pyridine; N-dodecane; acetonitrile T=50°C; 3 h; Title compound not separated from byproducts;
参考文献
Synlett, , # 6 p. 881 - 884
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I); di-tert-butyl peroxide; triphenylphosphine in benzene T=150°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Chemical Communications, , vol. 47, # 7 p. 2161 - 2163
反应条件
copper(l) iodide; palladium diacetate; sodium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=100°C; 12 h; Inert atmosphere;
参考文献
Zhu, Daqian; Wu, Yongcheng; Wu, Baojian; Luo, Bingling; Ganesan; Wu, Fu-Hai; Pi, Rongbiao; Huang, Peng; Wen, Shijun
Organic Letters, 2014 , vol. 16, # 9 p. 2350 - 2353
反应条件
methanol; magnesium; palladium on activated charcoal T=20°C; 24 h;
参考文献
Chemistry - A European Journal, , vol. 13, # 5 p. 1432 - 1441
反应条件
copper(l) iodide; palladium diacetate; sodium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=100°C; 12 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 16, # 9 p. 2350 - 2353
反应条件
Ni(PPh3)n; tetrabutylammomium bromide in N,N-dimethyl-formamide T=65°C; 21.5 h; electrochemical reduction;
参考文献
Tetrahedron Letters, , vol. 21, p. 631 - 634