联苯-4,4-二羧酸二甲酯合成路线 (共 64 条)
反应条件
caesium carbonate; hydroquinone; palladium diacetate in N,N-dimethyl acetamide T=75°C; Ullmann coupling; 2 h;
参考文献
Hennings, D. David; Iwama, Tetsuo; Rawal, Viresh H.
Organic Letters, 1999 , vol. 1, # 8 p. 1205 - 1208
反应条件
pyridine; manganese; FeBr2; cobalt(II) dibromide in acetonitrile T=50°C; 24 h;
参考文献
Organic Letters, , vol. 5, # 7 p. 1043 - 1045
反应条件
N-[(1E,2E)-2-(2,6-dimethylphenyl)ethylidene]-2,6-dimethylphenylamine; niobium bromide; zinc in tetrahydrofuran T=70°C; 10 h; Inert atmosphere;
参考文献
Valaeva; Asachenko; Kulyabin; Flid; Voskoboinikov
Russian Journal of Organic Chemistry, 2011 , vol. 47, # 11 p. 1774 - 1776
反应条件
palladium diacetate; cesium fluoride; 2-dicyclohexylphosphino-1,1'-biphenyl in 1,4-dioxane T=25°C; Inert atmosphere;
参考文献
Wilson, Daniela A.; Wilson, Christopher J.; Rosen, Brad M.; Percec, Virgil
Organic Letters, 2008 , vol. 10, # 21 p. 4879 - 4882
反应条件
tetraethylammonium iodide; zinc; NiCl2((PPh3)P)2 in tetrahydrofuran T=67°C; 10 h;
参考文献
Percec, Virgil; Bae, Jin-Young; Hill, Dale H.
Journal of Organic Chemistry, 1995 , vol. 60, # 4 p. 1060 - 1065
反应条件
potassium phosphate; Ni(COD)2; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 8 h; Inert atmosphere;
参考文献
THE TRUSTEES OF THE UNIVERSITY OF PENNSYLVANIA
Patent: WO2009/137322 A2, 2009 ;
Location in patent: Page/Page column 21; 29 ;
反应条件
manganese; cobalt (II) bromide; triphenylphosphine; trifluoroacetic acid in pyridine; N,N-dimethyl-formamide T=50°C;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 11 p. 2089 - 2092
反应条件
copper(l) chloride in methanol T=25°C; 4 h;
参考文献
Cheng, Guanjun; Luo, Meiming
European Journal of Organic Chemistry, 2011 , # 13 p. 2519 - 2523
反应条件
manganese; cobalt (II) bromide; triphenylphosphine; trifluoroacetic acid in pyridine; N,N-dimethyl-formamide T=50°C;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 11 p. 2089 - 2092
反应条件
manganese; cobalt (II) bromide; triphenylphosphine; trifluoroacetic acid in pyridine; N,N-dimethyl-formamide T=50°C;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 11 p. 2089 - 2092