1 -甲基-1H-吡唑-3-腈合成路线 （共 6 条）
反应条件
trichlorophosphate in pyridine T=-5°C; 2 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1209 - 1216
反应条件
1: 86 percent / cc. aq. ammonium hydroxide / Ambient temperature 2: 85 percent / phosphoryl chloride / pyridine / 2 h / -5 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1209 - 1216
反应条件
in acetonitrile Irradiation;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 12 p. 604 - 606
反应条件
magnesium 1) ether, 2) ether, 30 min, reflux; Yield given. Multistep reaction;
参考文献
Manaev, Yu. A.; Khrapov, A. V.; Perevalov, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 6 p. 656 - 658
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , vol. 27, # 6 p. 833 - 835
反应条件
1: 1) Mg / 1) ether, 2) ether, 30 min, reflux 2: 76 percent / HNO3 (d=1.51), Ac2O / 3 h / 65 - 70 °C View Scheme
参考文献
Manaev, Yu. A.; Khrapov, A. V.; Perevalov, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 6 p. 656 - 658
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , vol. 27, # 6 p. 833 - 835
反应条件
in acetonitrile
Irradiation;
参考文献
Barltrop, John A.; Day, A. Colin; Mack, Arthur G.; Shahrisa, Aziz; Wakamatsu, Shigeru
Journal of the Chemical Society, Chemical Communications, 1981 , # 12 p. 604 - 606
