potassium-sodium in ethylene glycol dimethyl ether
T=0°C; 3 h; Title compound not separated from byproducts;
参考文献
Collins, Clair J.; Hombach, Hans-Peter; Maxwell, Brian; Woody, Madge C.; Benjamin, Ben M.
Journal of the American Chemical Society, 1980 , vol. 102, # 2 p. 851 - 853
Collins, Clair J.; Hombach, Hans-Peter; Maxwell, Brian E.; Benjamin, Ben M.; McKamey, Donna
Journal of the American Chemical Society, 1981 , vol. 103, # 5 p. 1213 - 1214
iodine
1.) THF, RT, 2.) a) -78 deg C, 3 h, b) RT, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rieke, Reuben D.; Schulte, Louis D.; Dawson, Bryan T.; Yang, Sheng Sbeng
Journal of the American Chemical Society, 1990 , vol. 112, # 23 p. 8388 - 8398
Collins, Clair J.; Hombach, Hans-Peter; Maxwell, Brian; Woody, Madge C.; Benjamin, Ben M.
Journal of the American Chemical Society, 1980 , vol. 102, # 2 p. 851 - 853
Collins, Clair J.; Hombach, Hans-Peter; Maxwell, Brian E.; Benjamin, Ben M.; McKamey, Donna
Journal of the American Chemical Society, 1981 , vol. 103, # 5 p. 1213 - 1214
potassium-sodium
1.) glyme, triglyme, 0 deg C, 3 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Collins, Clair J.; Hombach, Hans-Peter; Maxwell, Brian; Woody, Madge C.; Benjamin, Ben M.
Journal of the American Chemical Society, 1980 , vol. 102, # 2 p. 851 - 853
Chel'tsova,M.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1965 , p. 107 - 115
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1965 , # 1 p. 124 - 133
