1,2,2,6,6-五甲基哌啶合成路线 (共 22 条)
反应条件
1: With N,N-dimethylthiocarbamoyl chloride in dichloromethane T=20°C; 2 h; 2: in acetonitrile 3 h; Reflux;
参考文献
Caliskan, Hafize; Zaim, Oemer
Synthetic Communications, 2010 , vol. 40, # 20 p. 3078 - 3083
反应条件
lithium aluminium tetrahydride in diethyl ether 0.5 h; Ambient temperature;
参考文献
Rae, Ian D.; Woolcock, Mark L.
Australian Journal of Chemistry, 1990 , vol. 43, # 2 p. 447 - 450
参考文献
Kostyanovskii, R. G.; Shakhgel'diev, M. A.; Nabiev, O. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 12 p. 2593
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 12 p. 2826 - 2827
反应条件
diethyl ether; ethanol; potassium carbonate
参考文献
Journal of the American Chemical Society, , vol. 79, p. 5279,5286
参考文献
Journal of the American Chemical Society, , vol. 79, p. 5439
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 4,4,5,5-tetramethyl-[1,3,2]dioxaborolane T=20°C; 7 h;
参考文献
Journal of the American Chemical Society, , vol. 134, # 42 p. 17384 - 17387
反应条件
ethylmagnesium bromide 1.) Et2O, reflux, 5 h, 2.) Et2O; Yield given. Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 68, # 5 p. 1401 - 1408
反应条件
in acetonitrile T=0°C; 6 h; UV-irradiation; Mechanism;
参考文献
Dalton Transactions, , vol. 41, # 46 p. 14046 - 14050
反应条件
in water T=6.5°C; Equilibrium constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1304 - 1308