1-(4-羟基-3-甲氧基苯基)-7-苯基庚烷-3-酮合成路线 （共 11 条）
反应条件
hydrogen; palladium on activated charcoal in benzene
参考文献
Itakawa,H.; Aiyama,R.
Phytochemistry (Elsevier), 1982 , vol. 21, p. 241
反应条件
1: 89 percent / 10percent KOH / ethanol / 13 h / Ambient temperature
2: 95 percent / H2 / 5percent Pd-C / methanol / 24 h / 760 Torr / Ambient temperature
View Scheme
参考文献
Itokawa,H.; Aiyama,R.
Phytochemistry (Elsevier), 1981 , vol. 20, p. 769
反应条件
1: 89 percent / 10percent KOH / ethanol / 13 h / Ambient temperature
2: 95 percent / H2 / 5percent Pd-C / methanol / 24 h / 760 Torr / Ambient temperature
View Scheme
参考文献
Itokawa,H.; Aiyama,R.
Phytochemistry (Elsevier), 1981 , vol. 20, p. 769
反应条件
1: 80 percent / HOAc, pyrrolidine / diethyl ether / 45 h / Ambient temperature
2: 98 percent / H2 / 5 percent Pd-C / benzene / 3 h
View Scheme
参考文献
Itakawa,H.; Aiyama,R.
Phytochemistry (Elsevier), 1982 , vol. 21, p. 241
反应条件
1: 10percent aq. NaOH / 3 h / Ambient temperature
2: H2 / 5percent Pd/C / CHCl3 / 9 h
3: 80 percent / acetic acid/pyrrolidine / diethyl ether
4: 98 percent / H2 / 5percent palladium-carbon / benzene
View Scheme
参考文献
Itokawa; Aiyama; Ikuta
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 7 p. 2491 - 2496
反应条件
1: H2 / 5percent Pd/C / CHCl3 / 9 h
2: 80 percent / acetic acid/pyrrolidine / diethyl ether
3: 98 percent / H2 / 5percent palladium-carbon / benzene
View Scheme
参考文献
Itokawa; Aiyama; Ikuta
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 7 p. 2491 - 2496
反应条件
1: tetrabutylammonium fluoride / tetrahydrofuran
2: H2 / Pd/C
View Scheme
参考文献
Lee, Hwa Jin; Kim, Ji Sun; Yoon, Joung Wha; Kim, Hee-Doo; Ryu, Jae-Ha
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 3 p. 377 - 379
反应条件
1: MnO2 / pentane
2: tetrabutylammonium fluoride / tetrahydrofuran
3: H2 / Pd/C
View Scheme
参考文献
Lee, Hwa Jin; Kim, Ji Sun; Yoon, Joung Wha; Kim, Hee-Doo; Ryu, Jae-Ha
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 3 p. 377 - 379
反应条件
1: imidazole
2: MnO2 / pentane
3: tetrabutylammonium fluoride / tetrahydrofuran
4: H2 / Pd/C
View Scheme
参考文献
Lee, Hwa Jin; Kim, Ji Sun; Yoon, Joung Wha; Kim, Hee-Doo; Ryu, Jae-Ha
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 3 p. 377 - 379
反应条件
1: MnO2 / pentane
2: tetrabutylammonium fluoride / tetrahydrofuran
3: H2 / Pd/C
View Scheme
参考文献
Lee, Hwa Jin; Kim, Ji Sun; Yoon, Joung Wha; Kim, Hee-Doo; Ryu, Jae-Ha
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 3 p. 377 - 379
