N-(1-甲基丙基)-N'-苯基苯-1,4-二胺合成路线 （共 5 条）
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; (Mor-DalPhos); sodium t-butanolate in toluene
T=110°C; 16 h; Inert atmosphere; chemoselective reaction;
参考文献
Tardiff, Bennett J.; McDonald, Robert; Ferguson, Michael J.; Stradiotto, Mark
Journal of Organic Chemistry, 2012 , vol. 77, # 2 p. 1056 - 1071
反应条件
platinum on activated charcoal; phosphoric acid
T=150°C; P=25742.8 Torr; Hydrogenation;
参考文献
du Pont de Nemours and Co.
Patent: US2734808 , 1951 ;
反应条件
platinum on activated charcoal
T=160°C; P=73550.8 Torr; Hydrogenation;
参考文献
ICI
Patent: US2822395 , 1955 ;
反应条件
in toluene
T=20°C; 0.5 h; Further byproducts given;
参考文献
Zapevalov, G. A.; Kuz'min, S. V.; Kogan, L. M.; Krol', V. A.
Doklady Chemistry, 1984 , vol. 274, p. 9 - 12
Doklady Akademii Nauk SSSR, 1984 , vol. 274, # 2 p. 335 - 338
反应条件
in toluene
T=20°C; 0.5 h; Further byproducts given;
参考文献
Zapevalov, G. A.; Kuz'min, S. V.; Kogan, L. M.; Krol', V. A.
Doklady Chemistry, 1984 , vol. 274, p. 9 - 12
Doklady Akademii Nauk SSSR, 1984 , vol. 274, # 2 p. 335 - 338
