4-(反式-4-n-丙基环己基)苯乙酮合成路线 （共 16 条）
反应条件
1: p-toluenesulfonic acid / toluene / Heating
2: H2 / 10percent Pd/C / ethanol
3: AlCl3 / 1,2-dichloro-ethane / 0.5 h
View Scheme
参考文献
Bezborodov, V. S.; Bubel', O. N.; Konovalov, V. A.; Ptashnikov, Yu. L.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1669 - 1674
反应条件
1: NaBH4 / propan-1-ol / 4 h / 30 - 35 °C
2: p-toluenesulfonic acid / toluene / Heating
3: H2 / 10percent Pd/C / ethanol
4: AlCl3 / 1,2-dichloro-ethane / 0.5 h
View Scheme
参考文献
Bezborodov, V. S.; Bubel', O. N.; Konovalov, V. A.; Ptashnikov, Yu. L.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1669 - 1674
反应条件
aluminium trichloride in 1,2-dichloro-ethane
0.5 h;
参考文献
Bezborodov, V. S.; Bubel', O. N.; Konovalov, V. A.; Ptashnikov, Yu. L.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1669 - 1674
反应条件
1: hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / or in 1:1 mixture of triethanolamine and glycerol
2: AlCl3 / 1,2-dichloro-ethane / 0.5 h
View Scheme
参考文献
Bezborodov, V. S.; Bubel', O. N.; Konovalov, V. A.; Ptashnikov, Yu. L.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1669 - 1674
反应条件
magnesium in tetrahydrofuran; diethyl ether
5 h; Heating; Yield given;
参考文献
Osman; Huynh-Ba
Molecular crystals and liquid crystals, 1984 , vol. 116, # 1-2 p. 141 - 152
反应条件
1: aq. NaOH, Br2 / dioxane / 3 h / 35 - 40 °C
2: SOCl2 / 1 h / Heating
View Scheme
参考文献
Bezborodov, V. S.; Bubel', O. N.; Konovalov, V. A.; Ptashnikov, Yu. L.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1669 - 1674
