反应条件
1: 1) LiAlH4, 2) 2N HCl, air / 1) Et2O, reflux, 2 h, 2) overnight 2: 79 percent / SOCl2, pyridine / CH2Cl2 / 4 h / Ambient temperature 3: 30 percent / K2CO3 / acetone; H2O / 48 h / Ambient temperature View Scheme
参考文献
Iwaoka, Michio; Tomoda, Shuji
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 67, # 1-4 p. 125 - 130
