N-亚苄基-4-甲氧基苯胺合成路线 (共 139 条)
反应条件
1: N-methylmorpholine / chlorobenzene / 0 - 5 °C 2: NaOH View Scheme
参考文献
Banik, Bimal K.; Manhas, Maghar S.
Tetrahedron, 2012 , vol. 68, # 52 p. 10769 - 10779
反应条件
1: phenyl-magnesium bromide With ZnCl2*TMEDA in tetrahydrofuran T=0°C; Inert atmosphere; 2: 4-methoxy-N-(phenylmethylene)-benzenamine With iron (III) acetylacetonate; 1,2-dichloro-2-methylpropane; 4,4'-di-tert-butyl-2,2'-dipyridyl in tetrahydrofuran T=0°C; 48 h; Inert atmosphere; 3: With hydrogenchloride; water in tetrahydrofuran T=20°C; 3 h; chemoselective reaction;
参考文献
Yoshikai, Naohiko; Matsumoto, Arimasa; Norinder, Jakob; Nakamura, Eiichi
Angewandte Chemie, International Edition, 2009 , vol. 48, # 16 p. 2925 - 2928
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate in toluene T=70°C; 24 h; Inert atmosphere;
参考文献
Li, Jianhui; Wang, Zhouyu; Jiang, Zhenju; Jiang, Shengqian; Xiong, Lilin
Asian Journal of Chemistry, 2011 , vol. 23, # 9 p. 4101 - 4103
反应条件
1: With titanium(IV) isopropylate in tetrahydrofuran T=0°C; 0.5 h; Inert atmosphere; 2: With phenyl silane in tetrahydrofuran T=20°C; 24 h; Inert atmosphere; diastereoselective reaction;
参考文献
European Journal of Organic Chemistry, , # 5 p. 951 - 959
反应条件
iron(III) chloride; phenylacetylene in acetonitrile 0.5 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 57, # 6 p. 1842 - 1848
反应条件
iron(III) chloride in acetonitrile 0.5 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 57, # 6 p. 1842 - 1848
反应条件
iron(III) chloride in acetonitrile 0.5 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 57, # 6 p. 1842 - 1848
反应条件
Co-phthalocyanine; (Ph)2SiH2 in ethanol T=70°C; 3 h;
参考文献
Kumar, Vishal; Sharma, Upendra; Verma, Praveen K.; Kumar, Neeraj; Singh, Bikram
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 5 p. 870 - 878
反应条件
in toluene
1 h; Ambient temperature;
参考文献
Hayes; Hayler; Walsgrove; Wicks
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 1 p. 209 - 212
反应条件
1: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chlorobenzene
T=20°C; 0.166667 h; Inert atmosphere;
2: With phenyl-magnesium bromide in anhydrous butyl ether; chlorobenzene
T=0°C; 3 h; Inert atmosphere;
参考文献
Muramatsu, Wataru; Nakano, Kimihiro; Li, Chao-Jun
Organic Letters, 2013 , vol. 15, # 14 p. 3650 - 3653