反应条件
1: Et3N / 1,2-dichloro-ethane / 20 °C
2: 1.027 g / SOCl2 / CH2Cl2; benzene / 4 h / 20 °C
3: 75 percent / diethyl ether / 24 h / 20 °C
4: 20 °C
5: NaOH / methanol; H2O / 12 h / Heating
6: 0.340 g / H2SO4 / 0.08 h / 20 °C
7: 66 percent / HBr; AcOH / 5 h / Heating
View Scheme
参考文献
Coelho, Paulo J.; Salvador, Maria A.; Oliveira, M. Manuel; Carvalho, Luis M.
Tetrahedron, 2004 , vol. 60, # 11 p. 2593 - 2599
