2,2-二甲基丙基次基膦合成路线 （共 36 条）
反应条件
selenium in toluene T=75°C; Cyclization; 96 h;
参考文献
Hitchcock; Nixon; Sakarya
Chemical Communications, 2000 , # 18 p. 1745 - 1746
参考文献
Regitz; Krill
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 115, p. 99 - 103
反应条件
tert-butyliminovanadium(V)-trichloride in toluene T=-78 - 25°C;
参考文献
Angewandte Chemie - International Edition, , vol. 37, # 9 p. 1233 - 1235
反应条件
1: (adamantyl)CP With tert-butyliminovanadium(V)-trichloride in toluene T=-78 - 25°C; 2: tert-butylphosphaethyne in toluene T=-78 - 25°C; Further stages. Title compound not separated from byproducts.;
参考文献
Chemistry - A European Journal, , vol. 6, # 24 p. 4558 - 4566
反应条件
1: With sulfur; tantalum thiochloride in toluene T=25°C; 10 h; 2: With triphenylphosphine in pentane T=20°C; 10 h;
参考文献
Dietz, Jochen; Schmidt, Thomas; Renner, Jens; Bergstraesser, Uwe; Tabellion, Frank; Preuss, Fritz; Binger, Paul; Heydt, Heinrich; Regitz, Manfred
European Journal of Organic Chemistry, 2002 , # 10 p. 1664 - 1676
反应条件
propanethial in toluene 4 h; UV-irradiation;
参考文献
D'Arbeloff-Wilson, Sarah E.; Hitchcock, Peter B.; Krill, Steffen; Nixon, John F.; Nyulaszi, Laszlo; Regitz, Manfred
Journal of the American Chemical Society, 2000 , vol. 122, # 19 p. 4557 - 4562
反应条件
in dichloromethane T=100°C; Condensation; 1 h; Title compound not separated from byproducts.;
参考文献
D'Arbeloff-Wilson, Sarah E.; Hitchcock, Peter B.; Krill, Steffen; Nixon, John F.; Nyulaszi, Laszlo; Regitz, Manfred
Journal of the American Chemical Society, 2000 , vol. 122, # 19 p. 4557 - 4562
反应条件
lt;(CO)Mn(Ph2PS)gt; in tetrahydrofuran T=50°C; 44 h;
参考文献
Lindner, Ekkehard; Haase, Cornelius; Mayer, Hermann A.; Kemmler, Martin; Fawzi, Riad; Steimann, Manfred
Angewandte Chemie, 1993 , vol. 105, # 10 p. 1521 - 1523
反应条件
T=120°C; 0.0833333 h;
参考文献
Wagner, Oliver; Ehle, Michael; Regitz, Manfred
Angewandte Chemie, 1989 , vol. 101, # 2 p. 227 - 229
参考文献
Wagner, Oliver; Ehle, Michael; Birkel, Manfred; Hoffmann, Juergen; Regitz, Manfred
Chemische Berichte, 1991 , vol. 124, # 5 p. 1207 - 1213
Title/Abstract Full Text Show Details
Wagner, Oliver; Ehle, Michael; Regitz, Manfred
Angewandte Chemie, 1989 , vol. 101, # 2 p. 227 - 229
