1,2,3,4-四氯-5,6-二硝基苯合成路线 (共 21 条)
反应条件
in dichloromethane; water 1 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1275 - 1278
反应条件
potassium fluoride in N,N-dimethyl-formamide T=130°C; 1 h; other solvents, times; also in the presence of phase transfer catalysts; Product distribution;
参考文献
Journal of Fluorine Chemistry, , vol. 81, # 2 p. 129 - 132
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide in diethyl ether; chloroform 24 h; Heating;
参考文献
Synthetic Communications, , vol. 15, # 6 p. 479 - 484
反应条件
potassium fluoride in N,N-dimethyl-formamide T=130°C; 1 h; other solvents, times; also in the presence of phase transfer catalysts; Product distribution;
参考文献
Heaton, Alan; Hill, Mark; Drakesmith, Frederick
Journal of Fluorine Chemistry, 1997 , vol. 81, # 2 p. 129 - 132
反应条件
in toluene 1 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 401 - 404
反应条件
dihydrogen peroxide; trifluoroacetic acid in chloroform
Heating;
参考文献
Berry,D.J. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 1285 - 1294
反应条件
dihydrogen peroxide; trifluoroacetic acid in chloroform
Heating;
参考文献
Berry,D.J. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 1285 - 1294
反应条件
2: H2O2, HCO2H / CHCl3
3: CF3CO2H, aq. H2O2 / CHCl3 / Heating
4: tetrahydrothiophene 1,1-dioxide
5: CF3CO2H, aq. H2O2 / CHCl3 / Heating
View Scheme
参考文献
Berry,D.J. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 1285 - 1294
反应条件
1: tetrahydrothiophene 1,1-dioxide
2: CF3CO2H, aq. H2O2 / CHCl3 / Heating
View Scheme
参考文献
Berry,D.J. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 1285 - 1294
反应条件
1: CF3CO2H, aq. H2O2 / CHCl3 / Heating
2: tetrahydrothiophene 1,1-dioxide
3: CF3CO2H, aq. H2O2 / CHCl3 / Heating
View Scheme
参考文献
Berry,D.J. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 1285 - 1294