反应条件
in water 50percent H3PO2 slowly added to 26percent aq. ammonia; soln. evapd., residue dissolved in hot MeOH, cooled, ether added with stirring, after a few hours ppt. filtered off and washed with ether, driedunder vac.;
参考文献
Yoshida, Yusuke; Inoue, Katsuya; Kyritsakas, Natalie; Kurmoo, Mohamedally
Inorganica Chimica Acta, 2009 , vol. 362, # 5 p. 1428 - 1434