2-甲基-1-丁烯-3-炔合成路线 （共 145 条）
反应条件
piperidine; copper(l) chloride in toluene
T=60°C; 5 h;
参考文献
Zheng, Qingwei; Hua, Ruimao; Wan, Youzhi
Applied Organometallic Chemistry, 2010 , vol. 24, # 4 p. 314 - 316
反应条件
piperidine; copper(l) chloride in toluene
T=60°C; 5 h;
参考文献
Zheng, Qingwei; Hua, Ruimao; Wan, Youzhi
Applied Organometallic Chemistry, 2010 , vol. 24, # 4 p. 314 - 316
反应条件
piperidine; copper(l) chloride in toluene
T=60°C; 5 h;
参考文献
Zheng, Qingwei; Hua, Ruimao; Wan, Youzhi
Applied Organometallic Chemistry, 2010 , vol. 24, # 4 p. 314 - 316
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in acetonitrile
T=80°C; Sonogashira Cross-Coupling; Sealed tube; Overall yield = 44 percentSpectr.;
参考文献
Buccini, Marco; Punch, Kathryn A.; Kaskow, Belinda; Flematti, Gavin R.; Skelton, Brian W.; Abraham, Lawrence J.; Piggott, Matthew J.
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 7 p. 1100 - 1113
反应条件
H2 in n-heptane
Ni complex refluxed with 1.5 molar excess of HC2C(=CH2)CH3 in heptane or octane under N2 or H2 with IR monitoring, cooled in inert atmosphere, treated with equimolar amts. of Fe complex in refluxing heptane under H2for 40 min; filtered under N2, evapd. (vac.), dissolved in CHCl3, chromd. (SiO2, light petroleum/Et2O), crystd. (satd. heptane/CHCl3);
参考文献
Marchino, Maria Luisa Nanni; Sappa, Enrico; Lanfredi, Anna Maria Manotti; Tiripicchio, Antonio
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 1541 - 1546
