sodium methylate in 1,4-dioxane; methanol
Heating;
参考文献
D'yakov, V. M.; Makarov, A. F.; Kir'yanova, A. N.; Chernyshev, A. E.; Bochkarev, V. N.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 3 p. 548 - 552,480 - 485
NaOH in water
byproducts: C2H5OH; heating of (CH3)2Si(OC2H5)2, (CH3)3Si(OC2H5) and an excess (50percent) of H2O in presence of NaOH; sepn. of C2H5OH by distn.; boiling of the residue with 20percent aq. HCl; further products;; distn.;;
参考文献
Hunter, M. J.; Warrick, E. L.; Hyde, J. F.; Currie, C. C.
Journal of the American Chemical Society, 1946 , vol. 68, p. 2284 - 2290
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Gmelin Handbook: Si: MVol.C, 103, page 282 - 285
tetrabutyl ammonium fluoride in dichloromethane
T=20°C; 16 h;
参考文献
Bassindale, Alan R.; Liu, Zhihua; Parker, David J.; Taylor, Peter G.; Horton, Peter N.; Hursthouse, Michael B.; Light, Mark E.
Journal of Organometallic Chemistry, 2003 , vol. 687, # 1 p. 1 - 11
