1,2-二(1,1’-二环己醇基)乙炔合成路线 （共 36 条）
反应条件
1: 1-ethynyl-cyclohexan-1-ol With ethylmagnesium bromide in tetrahydrofuran T=23 - 80°C; 2: cyclohexanone in tetrahydrofuran T=23 - 25°C; 3: With ammonium chloride in tetrahydrofuran; water
参考文献
Ji, Ke-Gong; Zhu, Hai-Tao; Yang, Fang; Shu, Xing-Zhong; Zhao, Shu-Chun; Liu, Xue-Yuan; Shaukat, Ali; Liang, Yong-Min
Chemistry - A European Journal, 2010 , vol. 16, # 21 p. 6151 - 6154
反应条件
1: acetylene With potassium tert-butylate in tetrahydrofuran 0.25 h; Inert atmosphere; 2: cyclohexanone in tetrahydrofuran T=20°C; 18.67 h; Inert atmosphere;
参考文献
Fallon, Thomas; Robinson, Diane E.J.E.; Willis, Anthony C.; Paddon-Row, Michael N.; Sherburn, Michael S.
Chemistry - A European Journal, 2010 , vol. 16, # 3 p. 760 - 765
反应条件
1: trans-1,2-dichloroethylene With n-butyllithium in tetrahydrofuran; hexane T=0°C; 2: cyclohexanone in tetrahydrofuran; hexane T=0°C; 3: cyclohexanone Further stages;
参考文献
Nagaki, Aiichiro; Matsuo, Chika; Kim, Songhee; Saito, Kodai; Miyazaki, Atsuo; Yoshida, Jun-Ichi
Angewandte Chemie - International Edition, 2012 , vol. 51, # 13 p. 3245 - 3248
反应条件
potassium hydroxide; diethyl ether Einleiten von Acetylen;
参考文献
Zhurnal Obshchei Khimii, , vol. 9, p. 1631
Chem. Zentralbl., , vol. 111, # I p. 695
Journal of the American Chemical Society, , vol. 63, p. 3348
Izv. Armjansk. Akad.Chem.Abstr., p. 121,132
Izv. Armjansk. Akad.Chem.Abstr., , p. 3394
参考文献
Zhurnal Obshchei Khimii, , vol. 9, p. 1631
Chem. Zentralbl., , vol. 111, # I p. 695
Zhurnal Obshchei Khimii, , vol. 15, p. 412,416
Chem.Abstr., , p. 4683
参考文献
DE636456 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 23, p. 126
反应条件
sodium hydroxide T=85°C; P=14710.2 Torr;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 596, p. 65
Acetylene Chemistry <New York 1949> S. 83
反应条件
diethyl ether anschliessendes Behandeln mit Cyclohexanon;
参考文献
Journal of the American Chemical Society, , vol. 58, p. 972,974
Journal of the American Chemical Society, , vol. 59, p. 2666,2667
反应条件
potassium hydroxide in diethyl ether Favorsky reaction;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 41, # 11 p. 1386 - 1389
反应条件
potassium hydroxide; diethyl ether T=10 - 12°C;
参考文献
Zhurnal Obshchei Khimii, , vol. 7, p. 956,957
Chem. Zentralbl., , vol. 108, # II p. 3153
