2,3-(亚甲二氧基)苯甲醛合成路线 （共 37 条）
反应条件
potassium carbonate; copper(II) oxide
参考文献
Rigby, James H.; Maharoof, Umar S. M.; Mateo, Mary E.
Journal of the American Chemical Society, 2000 , vol. 122, # 28 p. 6624 - 6628
反应条件
caesium carbonate in N,N-dimethyl-formamide T=110°C; 2 h;
参考文献
Zelle; McClellan
Tetrahedron Letters, 1991 , vol. 32, # 22 p. 2461 - 2464
反应条件
hydrogen; potassium carbonate; palladium on activated charcoal in ethanol Catalytic hydrogenation; 3 h;
参考文献
Mattson, Ronald J.; Sloan, Charles P.; Lockhart, Christopher C.; Catt, John D.; Gao, Qi; Huang, Stella
Journal of Organic Chemistry, 1999 , vol. 64, # 21 p. 8004 - 8007
参考文献
US5389638 A1, ;
US 5389638 A
反应条件
caesium carbonate in N,N-dimethyl-formamide T=20 - 110°C;
参考文献
Tetrahedron, , vol. 59, # 24 p. 4383 - 4387
反应条件
potassium carbonate in N-methyl-acetamide; ice-water; dichloromethane
反应条件
potassium carbonate in N,N-dimethyl-formamide T=70°C; 16 h;
参考文献
Grudzien, Krzysztof; Malinska, Maura; Barbasiewicz, Michal
Organometallics, 2012 , vol. 31, # 9 p. 3636 - 3646
反应条件
1: 49 percent / acid 2: 67 percent / cupric oxide View Scheme
参考文献
Agricultural and Biological Chemistry, , vol. 44, # 2 p. 235 - 243
反应条件
sodium hydroxide; {[bis(trisubstituted benzyl)(2-pyridylmethyl)amine]Cu(OAc)} in acetonitrile T=20°C; 24 h;
参考文献
Dalton Transactions, , # 21 p. 2818 - 2824
反应条件
1.1: LiTMP / tetrahydrofuran / 0.67 h / -78 °C 1.2: 56 percent / tetrahydrofuran / -78 - 20 °C 2.1: 92 percent / hydrogen; potassium carbonate / Pd/C / ethanol / 3 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 64, # 21 p. 8004 - 8007
