L-2-((三氟甲基磺酰基)氧基)丙酸乙酯合成路线 （共 12 条）
反应条件
tetrabutylammonium fluoride hydrofluoride in dichloromethane T=20°C;
参考文献
Kim, Kyu-Young; Bong, Chan Kim; Hee, Bong Lee; Shin, Hyunik
Journal of Organic Chemistry, 2008 , vol. 73, # 20 p. 8106 - 8108
反应条件
in acetonitrile T=0 - 20°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 49, # 3 p. 449 - 454
反应条件
in acetonitrile T=20°C; 12 h;
参考文献
Tetrahedron Letters, , vol. 49, # 3 p. 449 - 454
反应条件
in acetonitrile T=20°C; 12 h;
参考文献
Tetrahedron Letters, , vol. 49, # 3 p. 449 - 454
反应条件
in acetonitrile T=20°C; 12 h;
参考文献
Tetrahedron Letters, , vol. 49, # 3 p. 449 - 454
反应条件
in acetonitrile T=20°C; 3 h; Yields of byproduct given;
参考文献
Burkard, Ulrike; Effenberger, Franz
Chemische Berichte, 1986 , vol. 119, # 5 p. 1594 - 1612
反应条件
1: K2CO3 / CH2Cl2 / 6 h / 20 °C 2: 81 percent / H2 / 30percent Pd/C / tetrahydrofuran; H2O; acetic acid / 20 °C / 735.5 Torr View Scheme
参考文献
Effenberger, Franz; Burkard, Ulrike
Liebigs Annalen der Chemie, 1986 , # 2 p. 334 - 358
反应条件
in dichloromethane T=20°C; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Effenberger, Franz; Burkard, Ulrike
Liebigs Annalen der Chemie, 1986 , # 2 p. 334 - 358
反应条件
1: rac-2-(Trifluormethylsulfonyloxy)propionsaeure-ethylester; acetonitrile With trimethylsilyl trifluoromethanesulfonate in acetonitrile T=130°C; Inert atmosphereMicrowave irradiationSealed tube; 2: acrylic acid With triethylamine in acetonitrile T=150°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Journal of Organic Chemistry, , vol. 79, # 3 p. 1303 - 1319
反应条件
Bis(3-morpholinylpropyl)phenylphosphine in dichloromethane
参考文献
Shiosaki, Kazumi; Fels, Gregor; Rapoport, Henry
Journal of Organic Chemistry, 1981 , vol. 46, # 16 p. 3230 - 3234
