in neat (no solvent) reaction of CsF and ClF3 at 80°C about 4 h; condensation of F2 to CsClF4; heating 22 h at 150°C; removing of excess F2; apparatus described;; distillation of ClF5;;
参考文献
Pilipovich, D.; Maya, W.; Lawton, E. A.; Bauer, H. F.; Sheehan, D. F.; et al.
Inorganic Chemistry, 1967 , vol. 6, p. 1918 - 1919
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Gmelin Handbook: Cl: SVol.B2, 121, page 573 - 575
chlorine in neat (no solvent)
Kinetics; addn. of Cl2 to - 130°C cooled O2F2;;
参考文献
Streng, A.
Journal of the American Chemical Society, 1963 , vol. 85, p. 1380 - 1385
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Gmelin Handbook: Cl: SVol.A, 152, page 355 - 358
