反应条件
aluminium trichloride; carbon in neat (no solvent) chlorinating of rare earth/carbon (molar ration 3/1) mixt. (Cl2 flow rate 20 ml/min, 800 K, 2 h), heating in CO/HCl flow (800-1200 K), chemical vapor transport (AlCl3, 1300 K, 6 h, CO carrier gas, 40 ml/min); atomic emission spectrometric monitoring;
参考文献
Journal of Alloys and Compounds, , vol. 287, # 1-2 p. 109 - 113