2-苯基[1,2,4]三唑并[1,5-a]吡啶合成路线 （共 9 条）
反应条件
bis-[(trifluoroacetoxy)iodo]benzene
T=20°C; 0.166667 h; Reagent/catalystSolventConcentration;
参考文献
Zheng, Zisheng; Ma, Shuangyu; Tang, Linlin; Zhang-Negrerie, Daisy; Du, Yunfei; Zhao, Kang
Journal of Organic Chemistry, 2014 , vol. 79, # 10 p. 4687 - 4693
反应条件
air; copper–zinc supported on Al2O3–TiO2 in 1,2-dichloro-benzene
T=140°C; 20 h; Green chemistry; Catalytic behavior; Reagent/catalystSolvent;
参考文献
Meng, Xu; Yu, Chaoying; Zhao, Peiqing
RSC Advances, 2014 , vol. 4, # 17 p. 8612 - 8616
反应条件
1: copper(l) iodide; 2,3'-bipyridine; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen; ammonium hydroxide / ethanol / 24 h / 20 °C
2: zinc(II) iodide / 1,2-dichloro-benzene / 24 h / 130 °C
View Scheme
参考文献
Yin, Weiyu; Wang, Chengming; Huang, Yong
Organic Letters, 2013 , vol. 15, # 8 p. 1850 - 1853
反应条件
in 1,2,3,4-tetrahydro-naphthalene
1 h; Heating;
参考文献
Rao, P. Jayaprasad; Reddy, K. Kondal
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, p. 117 - 120
反应条件
1: 87 percent / Schotten-Baumann
2: 90 percent / sodium carbonate / ethanol; H2O / 1 h / Heating
3: PCl5 / 1 h / 100 °C
4: sodium azide, sodium acetate / H2O; acetone / 12 h
5: 67 percent / 1,2,3,4-tetrahydro-naphthalene / 1 h / Heating
View Scheme
参考文献
Rao, P. Jayaprasad; Reddy, K. Kondal
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, p. 117 - 120
反应条件
1: sodium azide, sodium acetate / H2O; acetone / 12 h
2: 67 percent / 1,2,3,4-tetrahydro-naphthalene / 1 h / Heating
View Scheme
参考文献
Rao, P. Jayaprasad; Reddy, K. Kondal
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, p. 117 - 120
反应条件
1: PCl5 / 1 h / 100 °C
2: sodium azide, sodium acetate / H2O; acetone / 12 h
3: 67 percent / 1,2,3,4-tetrahydro-naphthalene / 1 h / Heating
View Scheme
参考文献
Rao, P. Jayaprasad; Reddy, K. Kondal
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, p. 117 - 120
反应条件
1: 90 percent / sodium carbonate / ethanol; H2O / 1 h / Heating
2: PCl5 / 1 h / 100 °C
3: sodium azide, sodium acetate / H2O; acetone / 12 h
4: 67 percent / 1,2,3,4-tetrahydro-naphthalene / 1 h / Heating
View Scheme
参考文献
Rao, P. Jayaprasad; Reddy, K. Kondal
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, p. 117 - 120
反应条件
1: 87 percent / Schotten-Baumann
2: 90 percent / sodium carbonate / ethanol; H2O / 1 h / Heating
3: PCl5 / 1 h / 100 °C
4: sodium azide, sodium acetate / H2O; acetone / 12 h
5: 67 percent / 1,2,3,4-tetrahydro-naphthalene / 1 h / Heating
View Scheme
参考文献
Rao, P. Jayaprasad; Reddy, K. Kondal
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, p. 117 - 120
