in solid other Radiation; placing metal in porcelain boat in flask with reactive gas and Ar; applying microwave power; further admitting gas as required; sublimation onto a cold finger in the flask; detn. by X-ray powder diffraction;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 2541 - 2544
in neat (no solvent) byproducts: H2; in a quartz tube heated to 22-25°C in a stream of Br2 in Ar; sublimation at 500°C, purity 99percent;
参考文献
Golovanova, A. I.; Konstantinova, A. I.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1985 , vol. 30, p. 320 - 321
Zhurnal Neorganicheskoi Khimii, 1985 , vol. 30, p. 566 - 567
