E. I. DU PONT DE NEMOURS AND COMPANY; NAPPA, Mario, Joseph; SWEARINGEN, Ekaterina, N.
Patent: WO2012/67864 A1, 2012 ;
Location in patent: Page/Page column 12-13 ;
in neat (no solvent)
slight excess over the stoich. amt. of COF2 required; reaction mixt. heated in a stainless steel or monel cylinder at 185°C for 12 h;
参考文献
Mallela, S. P.; Gupta, O. D.; Shreeve, Jean'ne M.
Inorganic Chemistry, 1988 , vol. 27, p. 208 - 209
in neat (no solvent)
heating in dry oxygen to 300°C;
参考文献
Ippolitov, E. G.; Tripol'skaya, T. A.; Zhigarnovskii, B. M.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1979 , vol. 24, p. 299 - 301
Zhurnal Neorganicheskoi Khimii, 1979 , vol. 24, p. 539 - 541
