反应条件
1: 1.) LDA / 1.) DME, -78 deg C, 10 min, 2.) -78 deg C -> 0 deg C, 25 min
2: 1.) m-CPBA, 2.) pyridine, 3.) Me2S, 4.) PhSH, NEt3
3: 88 percent / AcOH / tetrahydrofuran; H2O / 7 h / 21 °C
View Scheme
参考文献
Reich, Hans J.; Shah, Shrenik K.; Gold Paul M.; Olson Richard E.
Journal of the American Chemical Society, 1981 , vol. 103, # 11 p. 3112 - 3120
