in perchloric acid addition of iodide to a solution of BiOClO4 in diluted HClO4 solution; formation of a mixture of BiI3 and BiOI (precipitation) and of BiI4(1-);; content of iodides depending on Bi : HClO4 ratio; X- ray spectroscopic determination;;
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), , vol. 34, p. 1276 - 1280
Zhurnal Neorganicheskoi Khimii, , vol. 34, p. 2244 - 2249
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反应条件
in neat (no solvent) iodination of grown films in a specially designed glass chamber, contained I-crystals, at 30°C, for 140 h; replacement of S is not completed;
参考文献
Physica Status Solidi (A) Applied Research, , vol. 105, # 2 p. 455 - 459