in neat (no solvent) byproducts: Mg(ClO4)2; at 130 °C predried Mg(ClO3)2 decomposed in mixture with 1/10 MgO at 320 °C with formation of MgCl2 and a very small amount of Mg(ClO4)2;;
1,1-dibromo ethane in tetrahydrofuran (Ar or vac.); a soln. of Sn compd. in THF kept over Mg turnings (preactivated with dibromoethane) at 293 K for 48 h under stirring;
参考文献
Russian Journal of General Chemistry, , vol. 74, # 7 p. 1101 - 1104
1,1-dibromo ethane in tetrahydrofuran (Ar or vac.); a soln. of Sn compd. in THF kept over Mg turnings (preactivated with dibromoethane) at 293 K for 48 h under stirring;
参考文献
Russian Journal of General Chemistry, , vol. 74, # 7 p. 1101 - 1104
