in neat (no solvent) inert condition; addn. of I2 to mixt. of Mg and Ga, heating in vac. (150°C), chilling, addn. of EtI (50 - 70°C, 1 h), heating (90 °C, 4 h); distillation;
参考文献
Zakharkin; Gavrilenko
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1999 , vol. 29, # 7 p. 1243 - 1247
in gaseous matrix CCl4 with helium was fed to MgO samples placed in a quartz reactor at a total flow rate of 30 mL/min after MgO were pretreated under helium flowat 723 K;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 77, # 6 p. 1239 - 1247
